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Comprehensive Organic Synthesis: Oxidation by Trost B.M., Fleming I., Ley S.V. (eds.) PDF

By Trost B.M., Fleming I., Ley S.V. (eds.)

ISBN-10: 0080405983

ISBN-13: 9780080405988

This quantity covers all tools of oxidation to be used in natural synthesis. Emphasis has been put on selectivity and practical crew compatibility including sensible software and purposes. the quantity is greatly divided to hide oxidation of unactivated carbon-hydrogen bonds, oxidation of activated carbon-hydrogen bonds, that's to claim these adjoining to activating substituents and adjoining to heteroatoms, and oxidation of carbon-carbon double bonds. the amount additionally covers oxidation of C-X bonds, carbon-carbon unmarried bonds, heteroatom oxidation and a few detailed subject matters reminiscent of electrochemical tools, oxidative rearrangements, good supported reagents, electron move oxidation, and organic equipment.

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1997, 38, 973. 6. ; Kogan, T. P. Tetrahedron Lett. 1997, 38, 4965. Solid-Phase Organic Syntheses: Volume One. Edited by Anthony W. Czarnik Copyright # 2001 John Wiley & Sons, Inc. ISBNs: 0-471-31484-6 (Hardback); 0-471-22043-4 (Electronic) CHAPTER FIVE SOLID-PHASE MANNICH REACTIONS OF A RESIN-IMMOBILIZED ALKYNE Submitted by SCOTT L. DAX and MARK A. YOUNGMAN Drug Discovery, The R. W. ) / DMF. b: 20 Eq. aldehyde, 10 Eq. amine, 5 Eq. 1,4-dimethylpiperazine, 1 Eq. Cu(I)Cl, dioxane, 75 C. c: TFA / DCM (1:3).

Lett. 1997, 7, 2331. 5. Katritzky, A. ; Pleynet, D. P. ; Yang, B. J. Org. Chem. 1997, 62, 4155; Xiao, X. ; Patel, D. V. J. Org. Chem. 1997, 62, 6968. 6. ; Kassir, J. M; Kogan T. P. J. Bioorg. Med. Chem. Lett. 1998, 8, 3043. 7. Carpino, L. ; Albericio, F. J. Chem. Soc. Chem. Commun. 1994, 201. 8. Ostresh, J. ; Winkle, J. ; Hamashin, V. ; Houghten, R. A. Biopolymers, 1994, 34, 1681. 9. ; Ralph, A. , J. Org. Chem. 1997, 62, 6090. 60 (s, 1H, NH) ppm. MS/EI (C19H28N4O3) calculated: 360, observed: 383 (þNa þ ).

0 m Eq/g) in DMF (100 mL) in a 500-mL Erlenmeyer flask. 3 mL, 30 mmol; note 1). The flask was flushed with N2, stoppered, and allowed to mix overnight on an orbital shaker (note 2). The mixture was then filtered and washed with the following solvents: 2 Â 9:1 DMF:H2O, 1 Â DMF, 1 Â DCM, 1 Â MeOH, 2 Â DMF, 2 Â DCM. A wash consisted of suspending the resin in the solvent ($50 mL), stirring or swirling, then filtering. 1 g. 9. 42%. NOTES 1. The reaction warms slightly after the addition of methanesulfonyl chloride.

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Comprehensive Organic Synthesis: Oxidation by Trost B.M., Fleming I., Ley S.V. (eds.)

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